Perilla leaves picked from four areas were used to assay the freezing point and contents of both solublesolids and water of its whole leaf. The relationship among them was also investigated to provide theory proof for peril-la leaf storage. The results showed that the water contents were from 72.16% to 85.81%, SSC were from 5.9 mg/g to 12.3 mg/g, and the freezing points were from-0.57℃ to-0.78℃. The freezing points was significant negatively cor-related with SSC, but it was not related to water content.