基于HS-SPME-GC-MS技术分析意大利葡萄果实香气
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S663.1

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天津市林果现代农业产业技术体系项目(ITTFPRS2018005);国家现代农业产业技术体系建设专项资金项目(CARS-29)


Analysis on Aroma Components of Grape Italia by HS-SPME-GC-MS
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    摘要:

    采用顶空固相微萃取(HS-SPME)及气相色谱-质谱技术(GC-MS),内标-标准曲线定量、气味活性值分析及果实香气轮廓分析等方法,对天津产区玫瑰香型葡萄品种意大利的果实香气成分进行分析,研究其风味特性。结果显示:共检测出43种香气化合物,主要成分为醇类、醛类、萜烯类和酯类化合物,其中以1-己醇、反式-2-己烯-1-醛、反式-2-己烯-1-醇、里那醇、乙酸乙酯和正己醛为主。其果实香气主要由12种活性呈香成分贡献,气味活性值由高到低依次为:里那醇、正己醛、反式-2-己烯-1-醛、1-辛烯-3-醇、苯乙醛、己酸乙酯、反式-2-己烯-1-醇、正庚醛、香茅醇、丁酸乙酯、1-己醇和香叶醇。香气轮廓直观地显示其果实香气主要由植物类、水果类、花卉类和脂肪类气味构成,4种气味系列强度较为均衡。

    Abstract:

    A comprehensive analysis of the aroma components of Italia grapes, a muscat-flavor grapes grown in Tianjin, was conducted using headspace solid phase micro-extraction(HS-SPME), gas chromatography-mass spectrometry(GC-MS), along with methods such as internal standard-standard curve quantification, odor activity value analysis and aroma profile analysis. The results showed that a total of 43 aroma components with alcohols, aldehydes, terpenes, and esters being the major components. The main compounds identified included 1-hexanol, trans-2-hexen-1-al, trans-2-hexen-1-ol, linalool, ethyl acetate, and hexanal. Odor activity value results showed that aroma of grape Italia was mainly contributed by 12 kinds of active aroma components, including linalool, hexanal,trans-2-hexen-1-al, 1-octen-3-ol, phenylacetaldehyde, ethyl hexanoate, trans-2-hexen-1-ol, heptanal, citronellol, ethyl butyrate, 1-hexanol and geraniol(OAV from high to low). The visualized aroma profile showed that aroma of grape Italia was composed of plants, fruits, flowers and fats flavor, with a balanced intensity across the four odor series.

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李凯,商佳胤,王学智,张娜,王超霞,王丹,张鹤,田淑芬.基于HS-SPME-GC-MS技术分析意大利葡萄果实香气[J].东北农业科学,2023,48(4):106-112.

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  • 收稿日期:2020-07-14
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  • 在线发布日期: 2024-10-24
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